in melt placing of mixt. of Al with SnF2 (molar ratio SnF2:Al=1.65) in Fluoroplast-4 ampule, closing by screwed stopper, exposition for 1.00 h at 250°C; various product ratio yields for various conditions; cooling, stirring up in water, collection, drying;
参考文献
Goryacheva; Rakov; Solov'ev
Russian Journal of Inorganic Chemistry, 2001 , vol. 46, # 7 p. 949 - 952
Straumanis, M. E.; Wang, Y. N.
Journal of the Electrochemical Society, 1955 , vol. 102, p. 304 - 310
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Gmelin Handbook: F: SVol.3, 2.1.13.8.3, page 289 - 292