反应条件
1: 96 percent / pyridine, 4-dimethylaminopyridine / CH2Cl2 / 18 h / Ambient temperature
2: 47 percent / phosphate buffer pH=7 / 48 h / Pseudomonas fluorescens lipase
3: 44 percent / aq. NaOH
4: 1.) oxalyl chloride, DMSO, 2.) triethylamine / 1.) CH2Cl2, -50 to -60 deg C, 15 min, 2.) -50 deg C, 5 min
View Scheme
参考文献
Jackson, P. Mark; Roberts, Stanley M.; Davalli, Silvia; Donati, Daniele; Marchioro, Carla; Perboni, Alcide; Proviera, Stefano; Rossi, Tino
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 16 p. 2029 - 2039
