3,3-二甲氧基丙酸甲酯合成路线 （共 56 条）
反应条件
sodium hydride 1.) dioxane, 50 deg C, 2.) reflux; Yield given. Multistep reaction;
参考文献
Winckelmann, Ib; Larsen, Erik H.
Synthesis, 1986 , # 12 p. 1041 - 1044
反应条件
sodium hydride
1.) dioxane, 50 deg C, 2.) reflux; Yield given. Multistep reaction;
参考文献
Winckelmann, Ib; Larsen, Erik H.
Synthesis, 1986 , # 12 p. 1041 - 1044
反应条件
sodium hydride
1.) dioxane, 50 deg C, 2.) reflux; Yield given. Multistep reaction;
参考文献
Winckelmann, Ib; Larsen, Erik H.
Synthesis, 1986 , # 12 p. 1041 - 1044
反应条件
titanium(IV) isopropylate in diethyl ether
T=25°C; Kulinkovich reaction; 18 h;
参考文献
Limbach, Michael; Dalai, Suryakanta; De Meijere, Armin
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 7 p. 760 - 766
反应条件
triethylsilane; 1,1,1,3,3,3-hexamethyl-disilazane; iron(II) sulfate in dichloromethane
T=20°C; 48 h;
参考文献
Yang, Bai-Ling; Tian, Shi-Kai
European Journal of Organic Chemistry, 2007 , # 28 p. 4646 - 4650
反应条件
hydrogenchloride
Hydrolysis;
参考文献
Gambacorta, Augusto; Farah, Mohamed Elmi; Tofani, Daniela
Tetrahedron, 1999 , vol. 55, # 43 p. 12615 - 12628
