3,3-二甲氧基丙酸甲酯合成路线 (共 56 条)
反应条件
methanesulfonic acid; Pd(OAc)2 on carbon; Pd(OAc)2 on carbon - molybdovanadophosphate; oxygen T=50°C; Oxidation; Addition; P=760.051 Torr; 8 h;
参考文献
Kishi, Arata; Sakaguchi, Satoshi; Ishii, Yasutaka
Organic Letters, 2000 , vol. 2, # 4 p. 523 - 525
反应条件
toluene-4-sulfonic acid in methanol 2.5 h; Heating;
参考文献
Torii, Sigeru; Inokuchi, Tsutomu; Kubota, Minoru
Journal of Organic Chemistry, 1985 , vol. 50, # 21 p. 4157 - 4160
反应条件
tributylphosphine in methanol T=20°C; 168 h;
参考文献
El'natanov, Yu. I.; Kostyanovskii, R. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 2 p. 302 - 311
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 2 p. 382 - 391
反应条件
toluene-4-sulfonic acid T=100°C; 2 h;
参考文献
Lounasmaa, Mauri; Hanhinen, Pirjo; Jokela, Reija
Tetrahedron, 1995 , vol. 51, # 31 p. 8623 - 8648
反应条件
carbon dioxide; oxygen; palladium dichloride T=80°C; P=105011 Torr; 15 h;
参考文献
Tetrahedron, , vol. 64, # 3 p. 508 - 514
反应条件
carbon dioxide; polystyrene-supported benzoquinone; oxygen; palladium diacetate; sodium acetate T=20 - 27°C; P=45003.6 Torr; 6 h;
参考文献
Tetrahedron, , vol. 62, # 42 p. 9846 - 9854
反应条件
carbon dioxide; oxygen; palladium dichloride T=50°C; P=105011 Torr; 6 h;
参考文献
Tetrahedron, , vol. 64, # 3 p. 508 - 514
反应条件
1: With sodium methylate in toluene T=15 - 30°C; Industrial scale; 2: With hydrogenchloride in water; toluene Industrial scale;
参考文献
Phillips, Gary; Fevig, Thomas L.; Lau, Patrick H.; Klemm, George H.; Mao, Michael K.; Ma, Chun; Gloeckner, James A.; Clark, Art S.
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 357 - 366
反应条件
silver trifluoromethanesulfonate T=70°C; 20 h;
参考文献
Chemistry Letters, , # 9 p. 727 - 728
反应条件
potassium carbonate 10 h; Ambient temperature;
参考文献
Tietze, Lutz-F.; Meier, Heinrich; Voss, Edgar
Synthesis, 1988 , # 4 p. 274 - 277