3-甲基-1,2-戊二烯合成路线 （共 15 条）
反应条件
lithium perchlorate in methanol electrochemical oxidation, 1.8 V; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 38, # 11 p. 1677 - 1682
反应条件
hydrogen; palladium on barium sulfate
参考文献
Crombie,L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1081 - 1090
反应条件
1: acetic acid; HBr 2: alcoholic potash View Scheme
参考文献
Ipatjew
Journal fuer Praktische Chemie (Leipzig), 1899 , vol. <2>59, p. 543
Journal fuer Praktische Chemie (Leipzig), 1900 , vol. 61, p. 126
反应条件
hydrogenchloride
und Eintragen des Reaktionsprodukts in eine Loesung von Lithiumalanat in siedendem Dioxan;
参考文献
Bailey; Pfeiffer
Journal of Organic Chemistry, 1955 , vol. 20, p. 95,100
反应条件
lithium aluminium tetrahydride in various solvent(s)
T=60°C; 1 h; Yield given;
参考文献
Meijer, J.; Ruitenberg, K.; Westmijze, H.; Vermeer, P.
Synthesis, 1981 , # 7 p. 551 - 554
反应条件
tri-n-butyl-tin hydride
参考文献
Fantazier,R.M.; Poutsma,M.L.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5490 - 5498
参考文献
Jacobs,T.L.; Johnson,R.N.
Journal of the American Chemical Society, 1960 , vol. 82, p. 6397 - 6404
反应条件
chloro-(2-methylpropyl)magnesium in diethyl ether
T=40°C; 20 h;
参考文献
Caporusso, Anna Maria; Lardicci, Luciano; Settimo, Federico da
Gazzetta Chimica Italiana, 1986 , vol. 116, # 10 p. 599 - 602
反应条件
in pentane
T=25°C; 6 h; Product distribution;
参考文献
Caporusso, Anna Maria; Lardicci, Luciano; Settimo, Federico da
Gazzetta Chimica Italiana, 1986 , vol. 116, # 10 p. 599 - 602
反应条件
in diethyl ether
T=40°C; 20 h; further temperature, further reaction time; Product distribution;
参考文献
Caporusso, Anna Maria; Lardicci, Luciano; Settimo, Federico da
Gazzetta Chimica Italiana, 1986 , vol. 116, # 10 p. 599 - 602
