反应条件
1: With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in tetrahydrofuran
T=-80 - 0°C; Inert atmosphere;
2: With boric acid trimethyl ester in tetrahydrofuran
T=-80 - 0°C; 3 h; Inert atmosphere;
3: With dihydrogen peroxide; acetic acid in tetrahydrofuran; water
T=0 - 20°C; Inert atmosphere;
参考文献
Kimachi, Tetsutaro; Torii, Eri; Ishimoto, Rina; Sakue, Ayako; Ju-ichi, Motoharu
Tetrahedron Asymmetry, 2009 , vol. 20, # 14 p. 1683 - 1689
