3-苯并[1,3]二氧杂环戊烯-5-基-1-(4-氟苯基)丙-2-烯-1-酮合成路线 （共 5 条）
反应条件
sodium hydroxide in ethanol
Claisen Schmidt condensation; Reflux;
参考文献
Insuasty, Braulio; Chamizo, Leidy; Munoz, Jhon; Tigreros, Alexis; Quiroga, Jairo; Abonia, Rodrigo; Nogueras, Manuel; Cobo, Justo
Archiv der Pharmazie, 2012 , vol. 345, # 4 p. 275 - 286
反应条件
1: potassium carbonate / acetonitrile / 24 h / |Reflux
2: potassium hydroxide / ethanol; water / 20 °C
View Scheme
参考文献
Wang, Hai-Hong; Qiu, Ke-Ming; Cui, Hong-En; Yang, Yu-Shun; Yin-Luo; Xing, Man; Qiu, Xiao-Yang; Bai, Li-Fei; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 2 p. 448 - 455
反应条件
1: potassium hydroxide / ethanol; water / 20 °C
2: potassium hydroxide / ethanol / 12 h / |Reflux
3: potassium carbonate / ethanol / 8 h / 80 °C
4: potassium hydroxide / ethanol; water / 20 °C
View Scheme
参考文献
Wang, Hai-Hong; Qiu, Ke-Ming; Cui, Hong-En; Yang, Yu-Shun; Yin-Luo; Xing, Man; Qiu, Xiao-Yang; Bai, Li-Fei; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 2 p. 448 - 455
反应条件
1: potassium hydroxide / ethanol / 12 h / |Reflux
2: potassium carbonate / ethanol / 8 h / 80 °C
3: potassium hydroxide / ethanol; water / 20 °C
View Scheme
参考文献
Wang, Hai-Hong; Qiu, Ke-Ming; Cui, Hong-En; Yang, Yu-Shun; Yin-Luo; Xing, Man; Qiu, Xiao-Yang; Bai, Li-Fei; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 2 p. 448 - 455
反应条件
1: potassium carbonate / ethanol / 8 h / 80 °C
2: potassium hydroxide / ethanol; water / 20 °C
View Scheme
参考文献
Wang, Hai-Hong; Qiu, Ke-Ming; Cui, Hong-En; Yang, Yu-Shun; Yin-Luo; Xing, Man; Qiu, Xiao-Yang; Bai, Li-Fei; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 2 p. 448 - 455
