(2R,3R,4S)-3-乙酰氨基-4-乙酰氧基-2-((1R,2R)-1,2,3-三乙酰氧基丙基)-3,4-二氢-2H-吡喃-6-羧酸甲酯合成路线 (共 94 条)
反应条件
in dichloromethane T=0 - 20°C; 48 h;
参考文献
Carbohydrate Research, , vol. 343, # 16 p. 2735 - 2739
反应条件
1: Amberlite IR120 (H+) 2: pyridine 3: triphenylphosphine hydrobromide / acetonitrile / 4 h / 60 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 7 p. 2418 - 2427
反应条件
4 A molecular sieve; silver trifluoromethanesulfonate in N,N-dimethyl-formamide Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 36, # 3 p. 914 - 919
反应条件
4 A molecular sieve; silver trifluoromethanesulfonate; 2',3'-O-diacetylinosine in N,N-dimethyl-formamide Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 36, # 3 p. 914 - 919
反应条件
4 A molecular sieve; silver trifluoromethanesulfonate; 2',3'-diacetyl-N4-benzoylcytidine in N,N-dimethyl-formamide Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 36, # 3 p. 914 - 919
反应条件
in acetonitrile T=20°C;
参考文献
Russian Chemical Bulletin, , vol. 54, # 2 p. 481 - 482
反应条件
1: Amberlite® IR 120-H / 20 °C / |Inert atmosphere 2: acetyl chloride; hydrogenchloride / 0 - 20 °C 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / benzene / 2 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 13 p. 3382 - 3386
Angew. Chem., , vol. 126, # 13 p. 3450 - 3454,5
反应条件
silver(I) salicylate in benzene 17 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 104, p. 221 - 234
反应条件
silver(I) salicylate in benzene 17 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 104, p. 221 - 234
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile 24 h; Title compound not separated from byproducts;
参考文献
Shpirt; Kononov; Torgov; Shibaev
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 717 - 719