4-甲基-5,5,5-三氟戊-1-烯-4-醇合成路线 （共 5 条）
反应条件
zinc in N,N-dimethyl-formamide
1 h; Ambient temperatureultrasonicated;
参考文献
Kitazume, Tomoya; Ishikawa, Nobuo
Chemistry Letters, 1981 , p. 1679 - 1680
反应条件
in diethyl ether
4 h; Ambient temperature;
参考文献
Camps; Coll; Messeguer; Pericas
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 1 p. 207 - 208
反应条件
zinc; bis(cyclopentadienyl)titanium dichloride in N,N-dimethyl-formamide
3 h; Irradiation;
参考文献
Kitazume, Tomoya; Ishikawa, Nobuo
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5186 - 5191
反应条件
bis-(2-hydroxy-ethyl)-amine
1.) from RT to 100 deg C, 3 h, 2) from 120 deg C to 160 deg C, 2 h; Multistep reaction;
参考文献
Zhou, Weike; Liang, Shaofang; Yu, Su; Luo, Weiming
Journal of Organometallic Chemistry, 1993 , vol. 452, # 1.2 p. 13 - 18
反应条件
hydrogenchloride; dimethylsulfide; ozone
1.) -70 deg C, methanol; 2.) 20 h, r.t.; Yield given. Multistep reaction;
参考文献
Camps; Coll; Messeguer; Pericas
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 1 p. 207 - 208
