2,4,5,7,9,10,12,14,15,17,19,20,21,22,23,24-十六碳硫杂-1,3,6,8,11,13,16,18-八硼杂五环[16.2.1.13,6.18,11.113,16]二十四烷合成路线 （共 2 条）
→
73825-17-92,4,5,7,9,10,12,14,15,17,19,20,21,22,23,24-十六碳硫杂-1,3,6,8,11,13,16,18-八硼杂五环[16.2.1.13,6.18,11.113,16]二十四烷
反应条件
in carbon disulfide
byproducts: CS2, HBr;
参考文献
Krebs, Bernt; Huerter, Hans-Ulrich
Angewandte Chemie, 1980 , vol. 92, p. 479 - 480
→
73825-17-92,4,5,7,9,10,12,14,15,17,19,20,21,22,23,24-十六碳硫杂-1,3,6,8,11,13,16,18-八硼杂五环[16.2.1.13,6.18,11.113,16]二十四烷
反应条件
a mixture of B2S3 and S in molar ratio 1:1.5 heated to ca. 300°C at ca. 1E-4 bar; pptd.; elem. anal.;
参考文献
Krebs, Bernt; Huerter, Hans-Ulrich
Angewandte Chemie, 1980 , vol. 92, p. 479 - 480
