愈创木酚基甘油-Β-愈创木基丙醚合成路线 （共 45 条）
反应条件
hydrogenchloride; 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; oxygen; nitric acid in water; acetonitrile
T=45°C; 24 h; High pressureSealed tube; chemoselective reaction;
参考文献
Rahimi, Alireza; Azarpira, Ali; Kim, Hoon; Ralph, John; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 17 p. 6415 - 6418
反应条件
Cα-dehydrogenase LigD in aq. buffer
T=60°C; pH=9; Enzymatic reaction; Kinetics;
参考文献
Reiter, Jochen; Strittmatter, Harald; Wiemann, Lars O.; Schieder, Doris; Sieber, Volker
Green Chemistry, 2013 , vol. 15, # 5 p. 1373 - 1381
反应条件
oxygen; salenCo(II) in chloroform
T=24.84°C; P=7500.75 Torr; 48 h; Product distribution;
参考文献
Canevali, Carmen; Orlandi, Marco; Pardi, Luca; Rindone, Bruno; Scotti, Roberto; Sipila, Jussi; Morazzoni, Franca
Journal of the Chemical Society, Dalton Transactions, 2002 , # 15 p. 3007 - 3014
反应条件
1: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
2: 96 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
2: 96 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
3: 52 percent / CuBr2 / ethyl acetate
4: 92 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
5: 90 percent / K2CO3 / dimethylsulfoxide / 0.17 h / 25 °C
6: O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
