愈创木酚基甘油-Β-愈创木基丙醚合成路线 （共 45 条）
反应条件
hydrogen in methanol T=150°C; P=15514.9 Torr; 2 h; Sealed tube;
参考文献
Parsell, Trenton H.; Owen, Benjamin C.; Klein, Ian; Jarrell, Tiffany M.; Marcum, Christopher L.; Haupert, Laura J.; Amundson, Lucas M.; Kenttaemaa, Hilkka I.; Ribeiro, Fabio; Miller, Jeffrey T.; Abu-Omar, Mahdi M.
Chemical Science, 2013 , vol. 4, # 2 p. 806 - 813
反应条件
hydrogen in ethylene glycol T=199.84°C; P=37503.8 Torr; Autoclave;
参考文献
Song, Qi; Wang, Feng; Xu, Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7019 - 7021
反应条件
10 palladium on activated charcoal; hydrogen in ethylene glycol T=199.84°C; P=37503.8 Torr; Autoclave;
参考文献
Song, Qi; Wang, Feng; Xu, Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7019 - 7021
反应条件
1: Cα-dehydrogenase LigD / aq. buffer / 60 °C / pH 9 / |Enzymatic reaction 2: β-etherase LigF / aq. buffer / 60 °C / pH 10 / |Enzymatic reaction 3: gluthione lyase LigG / aq. buffer / 60 °C / pH 7 / |Enzymatic reaction View Scheme
参考文献
Reiter, Jochen; Strittmatter, Harald; Wiemann, Lars O.; Schieder, Doris; Sieber, Volker
Green Chemistry, 2013 , vol. 15, # 5 p. 1373 - 1381
反应条件
sodium hydroxide; 9,10-dihydroxy anthracene in 1,4-dioxane; water T=140°C; 3 h; other time, other reagent; Product distribution;
参考文献
Brunow, Goesta; Poppius, Kristiina
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 6 p. 377 - 380
反应条件
hydrogenchloride; 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; oxygen; nitric acid in water; acetonitrile T=45°C; 24 h; High pressureSealed tube; chemoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 135, # 17 p. 6415 - 6418
反应条件
1: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation 2: 99 percent / pyridine / 0.17 h / 5 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 23 p. 7877 - 7888
反应条件
oxygen; rose bengal in acetonitrile
T=13°C; Irradiation;
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
buffer citrate phosphate; dihydrogen peroxide; benzotriazol-1-ol; Mn(TMePyP) immobilized on clay montmorillonite in 1,4-dioxane
T=60°C; pH=6; 4 h; Further byproducts given;
参考文献
Crestini, Claudia; Pastorini, Alessandra; Tagliatesta, Pietro
European Journal of Inorganic Chemistry, 2004 , # 22 p. 4477 - 4483
反应条件
buffer citrate phosphate; dihydrogen peroxide; benzotriazol-1-ol; Mn(TMePyP) immobilized on clay montmorillonite in 1,4-dioxane
T=60°C; pH=6; 4 h; Further byproducts given;
参考文献
Crestini, Claudia; Pastorini, Alessandra; Tagliatesta, Pietro
European Journal of Inorganic Chemistry, 2004 , # 22 p. 4477 - 4483
