愈创木酚基甘油-Β-愈创木基丙醚合成路线 （共 45 条）
反应条件
sodium tetrahydroborate in ethanol T=5 - 25°C; 3 h;
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 73 percent / anh. potassium carbonate / ethanol / 4 h / Heating 2: 80 percent / bromine / ethanol / 2 h / Ambient temperature 3: 83 percent 4: 91 percent 5: 1.) NaBH4; 2.) H2 / 1.) dioxane; 2.) ethanol View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 52, # 11 p. 1338 - 1342
反应条件
1: 80 percent / bromine / ethanol / 2 h / Ambient temperature 2: 83 percent 3: 91 percent 4: 1.) NaBH4; 2.) H2 / 1.) dioxane; 2.) ethanol View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 52, # 11 p. 1338 - 1342
反应条件
1: 83 percent 2: 91 percent 3: 1.) NaBH4; 2.) H2 / 1.) dioxane; 2.) ethanol View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 52, # 11 p. 1338 - 1342
反应条件
1: 91 percent 2: 1.) NaBH4; 2.) H2 / 1.) dioxane; 2.) ethanol View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 52, # 11 p. 1338 - 1342
反应条件
1: potassium carbonate; sodium hydroxide / dimethyl sulfoxide / 26.84 °C 2: sodium tetrahydroborate / ethanol / 26.84 °C View Scheme
参考文献
Catalysis Communications, , vol. 12, # 11 p. 993 - 995
反应条件
1: N,N-dimethyl-formamide / 26.84 °C 2: potassium carbonate; sodium hydroxide / dimethyl sulfoxide / 26.84 °C 3: sodium tetrahydroborate / ethanol / 26.84 °C View Scheme
参考文献
Catalysis Communications, , vol. 12, # 11 p. 993 - 995
反应条件
1.1: sodium / ethanol 1.2: Cooling with ice 2.1: potassium carbonate / ethanol / 2 h / 49.84 °C 3.1: sodium tetrahydroborate; sodium hydroxide / 20 °C View Scheme
参考文献
Chemical Communications, , vol. 48, # 56 p. 7019 - 7021
反应条件
1: potassium carbonate / ethanol / 2 h / 49.84 °C 2: sodium tetrahydroborate; sodium hydroxide / 20 °C View Scheme
参考文献
Chemical Communications, , vol. 48, # 56 p. 7019 - 7021
参考文献
Tetrahedron Letters, , vol. 43, # 32 p. 5669 - 5671
