1-甲氧基-4-苯基乙炔苯合成路线 （共 169 条）
反应条件
tetrabutyl ammonium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran
T=60°C; 48 h;
参考文献
Rossi, Renzo; Carpita, Adriano; Messeri, Tommaso
Gazzetta Chimica Italiana, 1992 , vol. 122, # 1 p. 65 - 72
反应条件
sodium hydroxide; copper(l) iodide in butan-1-ol
24 h; Heating;
参考文献
Kang, Suk-Ku; Yoon, Seok-Keun; Kim, Young-Mook
Organic Letters, 2001 , vol. 3, # 17 p. 2697 - 2699
反应条件
sodium hydroxide; copper(l) iodide in butan-1-ol
24 h; Heating;
参考文献
Kang, Suk-Ku; Yoon, Seok-Keun; Kim, Young-Mook
Organic Letters, 2001 , vol. 3, # 17 p. 2697 - 2699
反应条件
bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether
12 h; Heating;
参考文献
Gelman, Dmitri; Tsvelikhovsky, Dmitry; Molander, Gary A.; Blum, Jochanan
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6287 - 6290
反应条件
dichloro bis(acetonitrile) palladium(II); nonafluoro-n-butanesulfonyl fluoride; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetonitrile
T=60°C; Sonogashira Cross-Coupling; 5 h; Inert atmosphere;
参考文献
Ikawa, Takashi; Saito, Kozumo; Akai, Shuji
Synlett, 2012 , vol. 23, # 15 p. 2241 - 2246
反应条件
copper(l) iodide; 8-hydroxy-quinoline; potassium carbonate in N,N-dimethyl-formamide
T=110°C; 24 h; Inert atmosphere; ConcentrationReagent/catalystSolventTemperatureTime;
参考文献
Yan, Hong; Lu, Linhua; Sun, Peng; Zhu, Yan; Yang, Hailong; Liu, Defu; Rong, Guangwei; Mao, Jincheng
RSC Advances, 2013 , vol. 3, # 2 p. 377 - 381
反应条件
sodium t-butanolate in benzene
T=55°C; Sonogashira Cross-Coupling; 1 h;
参考文献
Scharf, Adam; Goldberg, Israel; Vigalok, Arkadi
Journal of the American Chemical Society, 2013 , vol. 135, # 3 p. 967 - 970
反应条件
pyrrolidine; Najera palladacycle I; 4-laurylbenzenesulfonic acid sodium salt; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water
T=130°C; Sonogashira Cross-Coupling; 0.5 h; Microwave irradiationSealed tubeGreen chemistry; chemoselective reaction;
参考文献
Buxaderas, Eduardo; Alonso, Diego A.; Najera, Carmen
European Journal of Organic Chemistry, 2013 , # 26 p. 5864 - 5870
反应条件
iodine in tetrahydrofuran
T=-78°C;
参考文献
Pelter, Andrew; Drake, Robert A.
Tetrahedron Letters, 1988 , vol. 29, # 33 p. 4181 - 4184
反应条件
bis-triphenylphosphine-palladium(II) chloride in dimethyl sulfoxide
0.05 h; microwave irradiation;
参考文献
Kakusawa, Naoki; Kurita, Jyoji
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 10 p. 1369 - 1371
