1-甲氧基-4-苯基乙炔苯合成路线 （共 169 条）
反应条件
potassium tert-butylate in tert-butyl alcohol
T=50°C; 5 h;
参考文献
Pati, Hari N.; Wicks, Martha; Holt Jr., Herman L.; LeBlanc, Regan; Weisbruch, Paul; Forrest, Lori; Lee, Moses
Heterocyclic Communications, 2005 , vol. 11, # 2 p. 117 - 120
反应条件
copper(l) iodide; [Pt(PPh3)4] in N,N-dimethyl-formamide
T=120°C; 14 h;
参考文献
Oh, Chang Ho; Reddy, V. Raghava
Synlett, 2004 , # 12 p. 2091 - 2094
反应条件
copper(l) iodide; [Pt(PPh3)4] in N,N-dimethyl-formamide
T=120°C; 12 h;
参考文献
Oh, Chang Ho; Reddy, V. Raghava
Synlett, 2004 , # 12 p. 2091 - 2094
反应条件
copper(l) iodide in ethylene glycol dimethyl ether; water
T=20°C; 3 h;
参考文献
Yu, Chan-Mo; Kweon, Jae-Hong; Ho, Pil-Su; Kang, Sin-Cheol; Lee, Gong Yeal
Synlett, 2005 , # 17 art. no. U23005ST, p. 2631 - 2634
反应条件
triethylamine; AgCl; palladium dichloride in acetonitrile
T=20°C; Sonogashira coupling; 0.333333 h;
参考文献
Zhu, Min; Zhou, Zhongshi; Chen, Rui
Synthesis, 2008 , # 17 art. no. P04108SS, p. 2680 - 2682
反应条件
bis-triphenylphosphine-palladium(II) chloride; ammonium hydroxide; hydroxylamine in N,N-dimethyl-formamide
T=20°C; Sonogashira coupling;
参考文献
Mohamed Ahmed, Mohamed S.; Kobayashi, Kei; Mori, Atsunori
Organic Letters, 2005 , vol. 7, # 20 p. 4487 - 4489
反应条件
copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride
T=80°C;
参考文献
Csekei, Marton; Novak, Zoltan; Kotschy, Andras
Tetrahedron, 2008 , vol. 64, # 6 p. 975 - 982
反应条件
1: methyl (2-phenylethynyl) sulfide With palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran
0.166667 h; Inert atmosphere;
2: 4-MeOC6H4ZnI*LiCl in tetrahydrofuran
T=25°C; 2 h; Inert atmosphere;
参考文献
Melzig, Laurin; Stemper, Jeremy; Knochel, Paul
Synthesis, 2010 , # 12 art. no. T04410SS, p. 2085 - 2091
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 12 h; Under air;
参考文献
Tang, Jian-Sheng; Tian, Mi; Sheng, Wen-Bing; Guo, Can-Cheng
Synthesis, 2012 , vol. 44, # 4 p. 541 - 546
反应条件
{(Pd{Fe(.eta.5-C5H5)(.eta.5-C5H3C(CH3)=NC6H4CH3-4)}(.mu.-Cl))2}; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetonitrile
T=110°C; 16 h; Inert atmosphere;
参考文献
Hu, Hao; Yang, Fan; Wu, Yangjie
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10506 - 10511
