1-甲氧基-4-苯基乙炔苯合成路线 （共 169 条）
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
反应条件
copper(l) iodide; 8-hydroxy-quinoline; sodium salt of phosphorous acid in ethanol
T=80°C; Suzuki coupling; 24 h;
参考文献
Wang, Shihua; Wang, Min; Wang, Lei; Wang, Bo; Li, Pinhua; Yang, Jin
Tetrahedron, 2011 , vol. 67, # 26 p. 4800 - 4806
反应条件
tetra(n-butyl)ammonium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran
T=20°C; Sonogashira-Hagihara coupling; 5 h;
参考文献
Chen, Gong; Zhu, Xinhai; Cai, Jiwen; Wan, Yiqian
Synthetic Communications, 2007 , vol. 37, # 8 p. 1355 - 1361
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=140°C; Sonogashira cross-coupling; 20 h;
参考文献
Feuerstein, Marie; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2004 , vol. 45, # 46 p. 8443 - 8446
反应条件
1: para-iodoanisole; trimethylsilylacetylene With potassium carbonate in methanol; acetonitrile
T=40°C; Sonogashira Cross-Coupling; 2 h;
2: iodobenzene in methanol; acetonitrile
T=40°C; Sonogashira Cross-Coupling; 2 h; chemoselective reaction;
参考文献
Mandali, Pavan Kumar; Chand, Dillip Kumar
Catalysis Communications, 2014 , vol. 47, p. 40 - 44
反应条件
potassium phosphate; copper(l) iodide; 8-hydroxy-quinoline in ethanol
T=100°C; Suzuki Coupling; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Liu, Jidan; Dai, Fenglin; Yang, Zhiyong; Wang, Sizhuo; Xie, Kai; Wang, Anwei; Chen, Xiang; Tan, Ze
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5678 - 5683
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=20°C; Hiyama Coupling; 12 h;
参考文献
Tang, Jiansheng; Guo, Cancheng
Journal of Chemical Research, 2014 , vol. 38, # 2 p. 123 - 127
反应条件
triethylamine; p-MeC6H4PdI(AsPh3)2
T=120°C; P=15200 Torr; 4 h;
参考文献
Kobayashi, Toshiaki; Tanaka, Masato
Journal of the Chemical Society, Chemical Communications, 1981 , # 7 p. 333 - 334
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=20°C; Hiyama Coupling; 12 h;
参考文献
Tang, Jiansheng; Guo, Cancheng
Journal of Chemical Research, 2014 , vol. 38, # 2 p. 123 - 127
反应条件
3C12H6N2O4(2-)*2Y(3+)*3Pd(2+)*6Cl(1-)*11H2O; 1,8-diazabicyclo[5.4.0]undec-7-ene in water
T=90°C; Sonogashira Cross-Coupling; 6 h;
参考文献
Huang, Jinping; Wang, Wei; Li, Hexing
ACS Catalysis, 2013 , vol. 3, # 7 p. 1526 - 1536
