3 -苄基-3-氮杂双环[3.1.0]己烷- 2.4 -二酮合成路线 （共 9 条）
反应条件
T=170°C; 1.5 h; Cooling with ice;
参考文献
F. HOFFMANN-LA ROCHE AG; HERMANN, Johannes Cornelius; KUGLSTATTER, Andreas; LUCAS, Matthew C.; PADILLA, Fernando; WANNER, Jutta; ZHANG, Xiaohu
Patent: WO2013/64445 A1, 2013 ;
Location in patent: Page/Page column 81 ;
反应条件
in neat (no solvent, solid phase) T=24.84°C; Photolysis;
参考文献
Photochemical and Photobiological Sciences, , vol. 11, # 12 p. 1929 - 1937
反应条件
in acetonitrile T=24.84°C; Photolysis;
参考文献
Photochemical and Photobiological Sciences, , vol. 11, # 12 p. 1929 - 1937
反应条件
1: SOCl2 / 1 h / Heating 2: Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 8 p. 2093 - 2096
反应条件
1: aq. NaOH / 5 h 2: SOCl2 / 1 h / Heating 3: Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 8 p. 2093 - 2096
反应条件
1: diethyl ether / 1 h 2: neat (no solvent, solid phase) / 24.84 °C / |Photolysis View Scheme
参考文献
Photochemical and Photobiological Sciences, , vol. 11, # 12 p. 1929 - 1937
反应条件
1: diethyl ether / 1 h 2: acetonitrile / 24.84 °C / |Photolysis View Scheme
参考文献
Photochemical and Photobiological Sciences, , vol. 11, # 12 p. 1929 - 1937
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in diethyl ether; toluene T=0°C; 4.5 h; Inert atmosphereReflux;
参考文献
F. HOFFMANN-LA ROCHE AG; HERMANN, Johannes Cornelius; KUGLSTATTER, Andreas; LUCAS, Matthew C.; PADILLA, Fernando; WANNER, Jutta; ZHANG, Xiaohu
Patent: WO2013/64445 A1, 2013 ;
Location in patent: Page/Page column 81 ;
