1,4-二(苯基)丁-2-炔-1-酮合成路线 (共 5 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine in tetrahydrofuran Ambient temperature;
参考文献
Jeevanandam; Narkunan; Ling
Journal of Organic Chemistry, 2001 , vol. 66, # 18 p. 6014 - 6020
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 40, # 26 p. 4841 - 4844
反应条件
manganese(IV) oxide in chloroform
Heating;
参考文献
Jeevanandam; Narkunan; Ling
Journal of Organic Chemistry, 2001 , vol. 66, # 18 p. 6014 - 6020
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: 71 percent / tetrahydrofuran; hexane / -78 - 25 °C
2.1: 80 percent / manganese dioxide / CHCl3 / Heating
View Scheme
参考文献
Jeevanandam; Narkunan; Ling
Journal of Organic Chemistry, 2001 , vol. 66, # 18 p. 6014 - 6020
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: 71 percent / tetrahydrofuran; hexane / -78 - 25 °C
2.1: 80 percent / manganese dioxide / CHCl3 / Heating
View Scheme
参考文献
Jeevanandam; Narkunan; Ling
Journal of Organic Chemistry, 2001 , vol. 66, # 18 p. 6014 - 6020