4-羟基苯并噁唑-2(3H)-硫酮合成路线 (共 4 条)
反应条件
in ethanol 3 h; Reflux;
参考文献
Rodgers, James D.; Shepard, Stacey; Arvanitis, Argyrios G.; Wang, Haisheng; Storace, Louis; Folmer, Beverly; Shao, Lixin; Zhu, Wenyu; Glenn, Joseph
Patent: US2010/298334 A1, 2010 ;
Location in patent: Page/Page column 120 ;
US 20100298334 A1
反应条件
1.1: boron tribromide / dichloromethane / 72 h / -45 - 20 °C / Inert atmosphere 1.2: pH 5 - 6 / Inert atmosphere; Cooling with ice 2.1: ethanol / 3 h / Reflux View Scheme
参考文献
US2010/298334 A1, ;
US 20100298334 A1
反应条件
methanol; carbon disulfide; potassium hydroxide
参考文献
Journal of Organic Chemistry, , vol. 19, p. 758,762, 765
参考文献
Journal of the Chemical Society, , vol. 125, p. 1704