2-[(8-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛基)氧基]-1,1,2,2-四氟乙烷磺酰氯合成路线 （共 3 条）
73606-15-22-[(8-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛基)氧基]-1,1,2,2-四氟乙烷磺酰氯
→
反应条件
1: 83.3 percent / KOH / H2O; ethanol / 8 h / Heating 2: 1.5 g / 2 h / 550 °C View Scheme
参考文献
Hu, Chang-Ming; Du, Xue-Mei; Zhou, Hui-Fen; Xu, Ze-Qi; Huang, Wei-Yuan
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 337 - 342
→
73606-15-22-[(8-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛基)氧基]-1,1,2,2-四氟乙烷磺酰氯
反应条件
potassium fluoride; chlorine in diethylene glycol dimethyl ether
1) 10 min, 2) 40 deg C, 6 h;
参考文献
Hu, Chang-Ming; Qing, Feng-Ling
Journal of Organic Chemistry, 1991 , vol. 56, # 22 p. 6348 - 6351
→
73606-15-22-[(8-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛基)氧基]-1,1,2,2-四氟乙烷磺酰氯
参考文献
anonymous
C.A., Huaxue Xuebao 37 (1978) 79 315/324 1980 , vol. 93, p. 113886
