2,4,6-三丁基环硼氧烷合成路线 (共 37 条)
反应条件
in water hydrolysis, determination of react.-enthalpy;;
参考文献
Mattraw, H. C.; Erickson, C. E.; Laubengayer, A. W.
Journal of the American Chemical Society, 1956 , vol. 78, p. 4901 - 4904
参考文献
McCusker, P. A.; Ashby, E. C.; Makowski, H. S.
Journal of the American Chemical Society, 1957 , vol. 74, p. 5182 - 5184
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Gmelin Handbook: B: B-Verb.9, 5.2.3, page 182 - 189
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McCusker, P. A.
Patent: GB854924 , 1960 ;
C. A., 1961 , vol. 1961, p. 15418
参考文献
US2943916 , ;
C. A., , p. 23224
反应条件
in neat (no solvent) byproducts: ethylene; at about 750°C;;
参考文献
Gmelin Handbook: B: B-Verb.13, 4.7.2, page 180 - 189
参考文献
Coffee,E.C.J.; Davies,A.G.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 1493 - 1496
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Grummit, O.
Journal of the American Chemical Society, 1962 , vol. 64, p. 1811 - 1814
反应条件
T=100 - 140°C; 5 h; Product distribution / selectivity;
参考文献
Nippon Aluminium Alkyls, Ltd.
Patent: EP1903047 A1, 2008 ;
Location in patent: Page/Page column 6 ;
参考文献
Snyder; Kuck; Johnson
Journal of the American Chemical Society, 1938 , vol. 60, p. 110
反应条件
aluminium trichloride P=0.05 Torr;
参考文献
Perrine; Keller
Journal of the American Chemical Society, 1958 , vol. 80, p. 1823,1825,1827
参考文献
Gmelin Handbook: B: B-Verb.13, 4.7.2.2, page 189 - 196
反应条件
in hexane boroxine was added under Ar to a soln. of AlCl3 in benzene with stirring;; volatiles removed in vac. at below 80 °C, the residue dissolved in pentane and crystd. at -78°C; elem. anal.;;
参考文献
Koester, Roland; Angermund, Klaus; Serwatowski, Janusz; Sporzynski, Andrzej
Chemische Berichte, 1986 , vol. 119, # 4 p. 1301 - 1314