1-(1-羟基-4-甲氧基-2-萘)-乙酮合成路线 (共 21 条)
参考文献
Zaveri, Nurulain; Chao, Wan-Ru
Patent: US2004/29914 A1, 2004 ;
反应条件
1: 60 percent / pyrrolidine / benzene / 48 h / Heating 2: 78 percent / Zn, HgCl2, aq. HCl / 3 h / Heating View Scheme
参考文献
Paradkar, Madhusudan V.; Godbole, Himanshu M.; Ranade, Anup A.; Joseph, Augustine R.
Journal of Chemical Research - Part S, 1998 , # 6 p. 318 - 319
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane; toluene
T=100°C; 6 h;
参考文献
Kobayashi, Shue; Moriwaki, Mitsuhiro; Hachiya, Iwao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 1 p. 267 - 273
反应条件
boron trifluoride diethyl etherate
T=120°C; Fries rearrangement; 0.0833333 h;
参考文献
Nguyen Van, Tuyen; Kesteleyn, Bart; De Kimpe, Norbert
Tetrahedron, 2001 , vol. 57, # 19 p. 4213 - 4219
反应条件
aluminium trichloride in 1,2-dichloro-ethane
T=60°C; 3 h;
参考文献
Rao, Rama A. V.; Deshpande, V. H.; Reddy, Laxma N.
Tetrahedron Letters, 1982 , vol. 23, # 42 p. 4373 - 4374
反应条件
aluminium trichloride in 1,2-dichloro-ethane
T=0°C; 6 h;
参考文献
Laatsch, Hartmut; Talvitie, Antti; Kral, Andreas; Ernst, Bernd-Peter; Noltemeyer, Mathias
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 2 p. 140 - 145
反应条件
in tetrahydrofuran
T=65°C; 5 h;
参考文献
Boger; Jacobson
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1919 - 1928
反应条件
boron trifluoride
Fries rearrangement; 1 h; Heating;
参考文献
Boyer, Jessica L.; Krum, Jodie E.; Myers, Michael C.; Fazal, Aleem N.; Wigal, Carl T.
Journal of Organic Chemistry, 2000 , vol. 65, # 15 p. 4712 - 4714
反应条件
in dichloromethane
T=0°C; 1 h;
参考文献
Shie, Tien-Lan; Lin, Chi-Hui; Lin, Shih-Lun; Yang, Ding-Yah
European Journal of Organic Chemistry, 2007 , # 29 p. 4831 - 4836
反应条件
scandium tris(trifluoromethanesulfonate) in toluene
T=100°C; 6 h;
参考文献
Kobayashi, Shue; Moriwaki, Mitsuhiro; Hachiya, Iwao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 1 p. 267 - 273