1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 50 °C 2.1: ammonium hydroxide / methanol / 100 °C 3.1: phosphorus tribromide / dichloromethane / 50 °C / Cooling with ice 3.2: 20 °C View Scheme
参考文献
Lin, Yih-Shyan; Park, Jaeok; De Schutter, Joris W.; Huang, Xian Fang; Berghuis, Albert M.; Sebag, Michael; Tsantrizos, Youla S.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 7 p. 3201 - 3215
1: With n-butyllithium; Di-n-butylmagnesium in tetrahydrofuran T=-10°C; Inert atmosphere; 2: With sulfuryl dichloride in tetrahydrofuran; toluene T=-10 - 10°C;