1,3-二甲基-5-异丙基巴比妥酸合成路线 (共 5 条)
反应条件
sulfuric acid; hydrogen; platinum on carbon in acetic acid
P=2585.74 Torr;
参考文献
Jursic, Branko S.; Neumann, Donna M.
Tetrahedron Letters, 2001 , vol. 42, # 25 p. 4103 - 4107
反应条件
1: N,N'-dimethyl-barbituric acid; acetone
2: With sulfuric acid; hydrogen; platinum on activated charcoal in water
P=3878.61 Torr; 48 h;
参考文献
Jursic, Branko S.; Stevens, Edwin D.
Tetrahedron Letters, 2003 , vol. 44, # 10 p. 2203 - 2210
反应条件
triethylamine in chloroform
T=20 - 25°C; 192 h;
参考文献
Krasnov, K. A.; Slesarev, V. I.; Artem'eva, Z. L.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 7.2 p. 1402 - 1405
Zhurnal Obshchei Khimii, 1989 , vol. 25, # 7 p. 1553 - 1557
反应条件
acetic anhydride; acetic acid
参考文献
Cope et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 356
反应条件
triethylamine in chloroform
T=20°C; Rate constant;
参考文献
Krasnov, K. A.; Slesarev, V. I.; Artem'eva, Z. L.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 7.2 p. 1402 - 1405
Zhurnal Obshchei Khimii, 1989 , vol. 25, # 7 p. 1553 - 1557