2,2’,3,6,6’-戊氯联苯合成路线 （共 6 条）
反应条件
1: 59 percent / Cu / 288 h / 230 °C
2: SO2Cl2, AlCl3 / CH2Cl2 / 1 h / Ambient temperature
View Scheme
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
1: 1.) NaNO2, aq. H2SO4, 2.) KI / 1.) 0-5 deg C, 10 min, 2.) 0 deg C, 15 min; r.t., 1 h
2: 59 percent / Cu / 288 h / 230 °C
3: SO2Cl2, AlCl3 / CH2Cl2 / 1 h / Ambient temperature
View Scheme
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane
1 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
poly(sodium styrenesulfonate-co-2-vinylnaphthalene) in water
24 h; Irradiationvar. time, solvent and concentration of HCB, several additional products; Product distributionMechanism;
参考文献
Nowakowska; Sustar; Guillet
Journal of the American Chemical Society, 1991 , vol. 113, # 1 p. 253 - 258
反应条件
sodium acetate; HNO2
Arylation; Gomberg-Bachman reaction;
参考文献
Bolgar; et al.
Chemosphere, 1995 , vol. 31, # 2 p. 2687 - 2705
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane
1 h; Ambient temperature; Product distribution;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
