6-氯-2-羟基喹啉-3-甲醛合成路线 （共 4 条）
反应条件
PPA
T=154 - 156°C; 0.166667 h;
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1520 - 1530
反应条件
hydrogenchloride
Heating;
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517
反应条件
1: 73 percent / phosphoryl chloride / 1 h / 75 °C / further reagents, further temperature
2: aq. 20percent sodium hydroxide / ethanol; H2O / 0.02 h / Heating
3: 94 percent / polyphosphoric acid / 0.17 h / 154 - 156 °C
View Scheme
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1520 - 1530
反应条件
1: aq. 20percent sodium hydroxide / ethanol; H2O / 0.02 h / Heating
2: 94 percent / polyphosphoric acid / 0.17 h / 154 - 156 °C
View Scheme
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1520 - 1530
