2,6-二氯喹啉-3-甲醛合成路线 （共 9 条）
反应条件
sodium lauryl sulfate; trichlorophosphate in acetonitrile Vilsmeier-Haack cyclisation; 1.5 h; Heating;
参考文献
Synlett, , # 2 p. 251 - 253
反应条件
hydrogenchloride; trichlorophosphate T=140°C; 2.2 h; further temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1520 - 1530
参考文献
Acta Poloniae Pharmaceutica - Drug Research, , vol. 68, # 2 p. 231 - 236
反应条件
trichlorophosphate T=75°C; 1 h; further reagents, further temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1520 - 1530
反应条件
1: hydroxylamine hydrochloride; sodium acetate 2: trichlorophosphate View Scheme
参考文献
Acta Poloniae Pharmaceutica - Drug Research, , vol. 68, # 2 p. 231 - 236
反应条件
1: acetic acid / |Reflux 2: trichlorophosphate / 24 h / 85 °C View Scheme
参考文献
Journal of the Brazilian Chemical Society, , vol. 25, # 2 p. 365 - 371
反应条件
sodium tetrahydroborate in methanol 0.5 h; Ambient temperature;
参考文献
Lavergne, Olivier; Lesueur-Ginot, Laurence; Rodas, Francesc Pla; Kasprzyk, Philip G.; Pommier, Jacques; Demarquay, Daniele; Prevost, Gregoire; Ulibarri, Gerard; Rolland, Alain; Schiano-Liberatore, Anne-Marie; Harnett, Jeremiah; Pons, Dominique; Camara, Jose; Bigg, Dennis C. H.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 27 p. 5410 - 5419
反应条件
hydrogen; sodium acetate; palladium dichloride in methanol T=35°C; P=760.051 Torr; 2 h;
参考文献
Chen, Xi-Bo; Hu, Qiu-Peng; Yuan, Qian-Jia; Ding, Wei; Ren, Jiangmeng; Zeng, Bu-Bing
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3798 - 3801
反应条件
hydrogenchloride
Heating;
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517
