N-[4-(4-乙酰氨基苯基)硫苯基]乙酰胺合成路线 （共 14 条）
反应条件
1: potassium dichromate; aqueous sulfuric acid; acetic acid 2: aqueous hydrochloric acid View Scheme
参考文献
Sasosow; Galtschenko
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1946 , vol. 19, p. 580,583, 584
Chem.Abstr., 1947 , p. 2703
参考文献
Merz; Weith
Chemische Berichte, 1871 , vol. 4, p. 394
反应条件
sulfuric acid in benzene
T=70 - 75°C; 2 h;
参考文献
Pilyugin; Kuznetsova; Sapozhnikov; Chikisheva; Kiseleva; Vorob'eva; Klimakova; Sapozhnikova; Davletov; Galeeva
Russian Journal of General Chemistry, 2008 , vol. 78, # 3 p. 446 - 450
反应条件
acetic acid; zinc
anschliessenden Erhitzen des Reaktionsgemisches mit Acetylchlorid;
参考文献
Sah; Fan; Pien
Journal of the Chinese Chemical Society (Peking), 1947 , vol. 15, p. 55,58, 60
Chem.Abstr., 1948 , p. 723
反应条件
acetic acid; zinc
anschliessenden Erhitzen des Reaktionsgemisches mit Acetylchlorid;
参考文献
Sah; Fan; Pien
Journal of the Chinese Chemical Society (Peking), 1947 , vol. 15, p. 55,58, 60
Chem.Abstr., 1948 , p. 723
反应条件
1: sodium sulfide; sulfur / water; N,N-dimethyl-formamide / 3 h / 110 °C
2: hydrogenchloride; iron / water; ethanol / 3 h / |Reflux
3: dichloromethane / 16 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Chen, Xiao Yun; Buschmann, Helmut; Bolm, Carsten
Synlett, 2012 , vol. 23, # 19 p. 2808 - 2810
参考文献
Hauptmann et al.
Justus Liebigs Annalen der Chemie, 1952 , vol. 576, p. 45,56
参考文献
Chandrasekaran, R.; Perumal, S.; Wilson, D.A.
Magnetic Resonance in Chemistry, 1987 , vol. 25, p. 1001 - 1006
反应条件
1: water; sodium sulfide
2: sulfur; sodium sulfide nonahydrate / 130 - 135 °C / Hydrogenation
3: ethanol / 40 °C
View Scheme
参考文献
Sasosow; Galtschenko
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1946 , vol. 19, p. 580,583, 584
Chem.Abstr., 1947 , p. 2703
参考文献
Merz; Weith
Chemische Berichte, 1871 , vol. 4, p. 394
