(Z)-1,1-二乙氧基-3-己烯合成路线 （共 3 条）
反应条件
bis(cyclopentadienyl)titanium dichloride; 2-methylpropylmagnesium bromide in diethyl ether T=20°C; Reduction; 48 h;
参考文献
Sha, Wei; Salomon, Robert G.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5315 - 5326
反应条件
1: 98 percent / n-BuLi; HMPA; CaCO3 / tetrahydrofuran; hexane / 66 h / -78 - 20 °C 2: 82 percent / i-BuMgBr; Cp2TiCl2 / diethyl ether / 48 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 17 p. 5315 - 5326
反应条件
perchloric acid in tetrahydrofuran 0.0166667 h; Yield given;
参考文献
Sha, Wei; Salomon, Robert G.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5315 - 5326
