4-溴-N,N-二甲基苯胺溴化镁合成路线 （共 37 条）
反应条件
magnesium in tetrahydrofuran T=80°C; 0.333333 h; microwave irradiation;
参考文献
Tetrahedron, , vol. 61, # 47 p. 11168 - 11176
参考文献
Tetrahedron, , vol. 69, # 5 p. 1526 - 1531
反应条件
iron(III) chloride; 1,2-dichloro-ethane in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Organic Letters, , vol. 7, # 10 p. 1943 - 1946
反应条件
1: p-toluidine With n-butyllithium; ZnCl2*TMEDA in tetrahydrofuran; hexane T=0 - 20°C; 0.5 h; Inert atmosphereSchlenk technique; 2: [4-(N,N-dimethylamino)-phenyl]-magnesium bromide With N,N'-dimethyl-N,N'-propyleneurea; bis(acetylacetonate)nickel(II); 1,2-dichloro-2-methylpropane in tetrahydrofuran; hexane T=0 - 20°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Organic Letters, , vol. 14, # 21 p. 5570 - 5573,4
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether T=20°C; 0.666667 h; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 1696 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1858 - 1865
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether T=20°C; 0.666667 h; Product distribution;
参考文献
Bumagin, N. A.; Kasatkin, A. N.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1696 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1858 - 1865
反应条件
C35H31BrN4NiP in tetrahydrofuran T=70°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1054 - 1061
反应条件
C35H31BrN4NiP in tetrahydrofuran T=25°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1054 - 1061
反应条件
iron (III) acetylacetonate in diethyl ether Inert atmosphere; Kinetics; Time;
参考文献
Hedstroem, Anna; Bollmann, Ulla; Bravidor, Jenny; Norrby, Per-Ola
Chemistry - A European Journal, 2011 , vol. 17, # 43 p. 11991 - 11993
