N-(乙氧基甲基)-N-乙基乙胺合成路线 (共 18 条)
反应条件
1: methyltrichlorosilane / acetonitrile / 0.08 h / 10 °C 2: acetonitrile / 0 °C View Scheme
参考文献
Rochin, C.; Babot, O.; Dunogues, J.; Duboudin, F.
Synthesis, 1986 , # 8 p. 667 - 668
反应条件
methyltrichloromonosilane in acetonitrile T=0°C; 42 h;
参考文献
Cooper, Mark S.; Fairhurst, Robin A.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1989 , vol. 45, # 4 p. 1155 - 1166
反应条件
zinc(II) chloride T=120°C;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 62, # 9 p. 2152 - 2154,1774 - 1775
反应条件
T=50°C; Acetylation; 2 h;
参考文献
Kachurin; Zaraiskii; Velichko; Zaraiskaya; Matvienko
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 8 p. 1117 - 1120
反应条件
hydrogenchloride; diethyl ether T=-15°C;
参考文献
Boehme; Ellenberg
Chemische Berichte, 1959 , vol. 92, p. 2976,2979
反应条件
1: methyltrichlorosilane / acetonitrile / 0.08 h / 10 °C
2: acetonitrile / 0 °C
View Scheme
参考文献
Rochin, C.; Babot, O.; Dunogues, J.; Duboudin, F.
Synthesis, 1986 , # 8 p. 667 - 668
反应条件
copper(l) iodide
Heating;
参考文献
Gevorkyan; Movsisyan; Dzhandzhulyan; Arakelyan; Petrosyan
Russian Journal of General Chemistry, 2008 , vol. 78, # 3 p. 504 - 505
反应条件
sulfur dioxide in acetonitrile
aminomethylation; 2 h; Heating;
参考文献
Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1997 , vol. 53, # 39 p. 13361 - 13372
反应条件
sulfur dioxide in acetonitrile
T=20°C; aminomethylation; 42 h;
参考文献
Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1997 , vol. 53, # 39 p. 13361 - 13372
反应条件
in acetonitrile
T=20°C; aminomethylation; 42 h;
参考文献
Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1997 , vol. 53, # 39 p. 13361 - 13372