4-氟-5-氧代-2,4-二(三氟甲基)-1,3-二氧戊环-2-羰基氟化物合成路线 （共 6 条）
反应条件
cesium fluoride in diethylene glycol dimethyl ether 2 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, # 2 p. 311 - 315
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 392 - 395
反应条件
cesium fluoride in diethylene glycol dimethyl ether
T=-35 - 20°C; 3.5 h;
参考文献
Sterlin; Avetisyan
Russian Chemical Bulletin, 2009 , vol. 58, # 6 p. 1318 - 1320
反应条件
1: α-(fluorosulfato)pentafluoroacetone With KHF2 in nitrobenzene
T=45 - 60°C; P=100 Torr;
2: With cesium fluoride in diethylene glycol dimethyl ether; bis [2-(2-methoxyethoxy)ethyl] ether
T=-32 - -30°C; 0.5 h;
3: hexafluorocyclopropylene oxide in diethylene glycol dimethyl ether; bis [2-(2-methoxyethoxy)ethyl] ether
T=-32 - -30°C; 2.5 h;
参考文献
Sterlin; Avetisyan
Russian Chemical Bulletin, 2009 , vol. 58, # 6 p. 1318 - 1320
反应条件
cesium fluoride in diethylene glycol dimethyl ether
T=20°C; P=3750.3 Torr; 0.166667 h;
参考文献
Yuminov, V. S.; Kartsov, S. V.; Vinogradov, L. E.; Fokin, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 2 p. 315 - 318
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 2 p. 396 - 398
反应条件
hydrogenchloride; N,N-dimethyl-formamide
1.) -30 deg C, 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Yuminov, V. S.; Kartsov, S. V.; Maksimov, V. L.; Fokin, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 2 p. 311 - 315
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 2 p. 392 - 395
反应条件
cesium fluoride in diethylene glycol dimethyl ether
2 h;
参考文献
Yuminov, V. S.; Kartsov, S. V.; Maksimov, V. L.; Fokin, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 2 p. 311 - 315
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 2 p. 392 - 395
