hydrogen; RhH(CO)(triphenylphosphine)3; (-)-DIPHOL in benzene T=52°C; P=25857.4 Torr; 192 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 45, # 11 p. 2145 - 2151
1: With bismuth trifluoromethanesulphonate; water in acetonitrile 1.5 h; 2: With 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; [bis(acetoxy)iodo]benzene; sodium hydrogencarbonate in acetonitrile T=20°C; 2 h;