1-(4-乙基氨基苯基)乙酮合成路线 (共 4 条)
反应条件
rhodium(III) 5,10,15,20-tetra(p-sulfonatophenyl)porphyrin; oxygen in methanol; water
T=90°C; P=760.051 Torr; 22 h;
参考文献
Ling, Zhen; Yun, Lin; Liu, Lianghui; Wu, Bing; Fu, Xuefeng
Chemical Communications, 2013 , vol. 49, # 39 p. 4214 - 4216
反应条件
1: acetyl chloride With aluminium trichloride in dichloromethane
T=0 - 5°C; 0.5 h;
2: N-ethyl-aniline in dichloromethane
T=0 - 20°C; 5 h;
参考文献
Singh, Sunil Kumar; Vobbalareddy, Saibaba; Kalleda, Srinivasa Rao; Rajjak, Shaikh Abdul; Casturi, Seshagiri Rao; Datla, Srinivasa Raju; Mamidi, Rao N.V.S.; Mullangi, Ramesh; Bhamidipati, Ravikanth; Ramanujam, Rajagopalan; Akella, Venkateswarlu; Yeleswarapu, Koteswar Rao
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2442 - 2450
反应条件
in water; dimethyl sulfoxide
T=90°C; 20 h;
参考文献
Abdellatif, Khaled R. A.; Chowdhury, Morshed A.; Knaus, Edward E.
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 6 p. 1707 - 1710
参考文献
Kumler
Journal of the American Chemical Society, 1946 , vol. 68, p. 1184,1188