反应条件
1: copper(l) iodide / tetrahydrofuran / -78 - 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h
3: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -60 - -50 °C
4: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol
View Scheme
参考文献
Gao, Yangguang; Shan, Qiuli; Liu, Jun; Wang, Linlin; Du, Yuguo
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 13 p. 2071 - 2079