(2E,4E)-2,4-癸二烯酸甲酯合成路线 (共 56 条)
参考文献
Crossley; Hilditch
Journal of the Chemical Society, 1949 , p. 3354
反应条件
sodium methylate
Yield given;
参考文献
Baeckstroem, Peter; Jacobsson, Ulla; Norin, Torbjoern; Unelius, C. Rikard
Tetrahedron, 1988 , vol. 44, # 9 p. 2541 - 2548
参考文献
Crombie et al.
Journal of the Chemical Society, 1955 , p. 1025
参考文献
Dolezal,S.
Collection of Czechoslovak Chemical Communications, 1972 , vol. 37, p. 3117 - 3121
反应条件
1: 8 percent KOH / ethanol / 4 h / Heating
2: oxalyl chloride / benzene / 1.) 30 min, room temperature; 2.) 30 min, reflux
3: 900 mg / diethyl ether / 1 h
View Scheme
参考文献
Burden,R.S.; Crombie,L.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2477 - 2481
反应条件
potassium hydroxide; di-p-nitrophenylphosphoric acid; tetrabutylammomium bromide
1.) methanol, 40 deg C, 2.) THF, 1 h, 3.) room temperature; Yield given. Multistep reaction;
参考文献
Jeffery, Tuyet
Synthetic Communications, 1988 , vol. 18, # 1 p. 77 - 84