1,4-二-叔丁基-2,5-二甲氧基苯合成路线 (共 26 条)
反应条件
in 1,2,2-trifluoro-trichloroethane
T=25°C; Product distributionRate constantMechanism;
参考文献
Zhao,C.X.; Jiang,X.K.
Journal of Fluorine Chemistry, 1985 , vol. 27, p. 401 - 410
反应条件
nitrogen(IV) oxide in dichloromethane
in the dark; -78 deg C, 2 min; RT, 15 min;
参考文献
Rathore; Bosch; Kochi
Tetrahedron, 1994 , vol. 50, # 23 p. 6727 - 6758
反应条件
in acetonitrile
T=25°C; 6.5 h; Irradiation;
参考文献
Svensson, Jan Olof
Acta Chemica Scandinavica, 1997 , vol. 51, # 1 p. 31 - 36
反应条件
nitrogen(IV) oxide in dichloromethane
T=-50°C; Irradiation;
参考文献
Svensson, Jan Olof
Acta Chemica Scandinavica, 1997 , vol. 51, # 1 p. 31 - 36
反应条件
in dichloromethane
T=-20°C; 1 h; Irradiation;
参考文献
Svensson, Jan Olof
Acta Chemica Scandinavica, 1997 , vol. 51, # 1 p. 31 - 36
反应条件
trifluoroacetic acid in dichloromethane
T=25°C; 1 h; Irradiationreaction temperature varied: -50 to 25 deg C; time: 0.25 to 6 h; solvent also acetonitrile; trifluoroacetic acid concn. 0-1.0 mol dm-3; nitration also by NO2 or HNO3; Product distributionMechanism;
参考文献
Svensson, Jan Olof
Acta Chemica Scandinavica, 1997 , vol. 51, # 1 p. 31 - 36