反应条件
1: 98 percent / K2CO3 / dimethylformamide / 0.08 h / 150 °C
2: 1.) dimethyldioxirane, 2.) p-TsOH / 1.) CH2Cl2, Me2CO, 0 deg C, 12 h, 2.) CH2Cl2, 0 deg C, 30 min
3: 100 percent / K2CO3 / acetone / 2 h / Heating
4: 100 percent / AlBr3 / acetonitrile / 0.83 h / 0 °C
5: 100 percent / H2 / 10percent Pd/C / ethyl acetate; methanol / Ambient temperature
View Scheme
参考文献
Horie, Tokunaru; Kitou, Takeshi; Kawamura, Yasuhiko; Yamashita, Kazuyo
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 4 p. 1033 - 1041
