5-苄基-2,4-二氨基嘧啶合成路线 （共 8 条）
反应条件
trichlorophosphate
dann mit aethanol.NH3 auf 155grad;
参考文献
Falco et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3758,3760
反应条件
1: MeONa / dimethylsulfoxide
2: HCl / propan-2-ol / Heating
3: 2.1 g / MeONa / ethanol / 36 h / Heating
View Scheme
参考文献
Otzen, Thomas; Wempe, Ellen G.; Kunz, Brigitte; Bartels, Rainer; Lehwark-Yvetot, Gudrun; Haensel, Wolfram; Schaper, Klaus-Juergen; Seydel, Joachim K.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 1 p. 240 - 253
反应条件
1: HCl / propan-2-ol / Heating
2: 2.1 g / MeONa / ethanol / 36 h / Heating
View Scheme
参考文献
Otzen, Thomas; Wempe, Ellen G.; Kunz, Brigitte; Bartels, Rainer; Lehwark-Yvetot, Gudrun; Haensel, Wolfram; Schaper, Klaus-Juergen; Seydel, Joachim K.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 1 p. 240 - 253
反应条件
sodium methylate in ethanol
36 h; Heating;
参考文献
Otzen, Thomas; Wempe, Ellen G.; Kunz, Brigitte; Bartels, Rainer; Lehwark-Yvetot, Gudrun; Haensel, Wolfram; Schaper, Klaus-Juergen; Seydel, Joachim K.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 1 p. 240 - 253
反应条件
ethanol; ammonia
T=100°C;
参考文献
Goldberg
Bulletin de la Societe Chimique de France, 1951 , p. 895,898
反应条件
2: POCl3
3: ethanol; NH3 / 100 °C
View Scheme
参考文献
Goldberg
Bulletin de la Societe Chimique de France, 1951 , p. 895,898
反应条件
1: POCl3
2: ethanol / 140 °C
View Scheme
参考文献
Goldberg
Bulletin de la Societe Chimique de France, 1951 , p. 895,898
反应条件
sulfuric acid; potassium nitrate
参考文献
Falco et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3758,3760
