N'-(3-苯基-2-丙烯亚基)-对甲苯磺酰肼合成路线 (共 6 条)
反应条件
dichloro bis(1,4-diazabicyclo[2.2.2]octane)(BH4)Zr(IV); toluene-4-sulfonic acid in sulfolane; N,N-dimethyl-formamide T=110°C; 7.3 h;
参考文献
Synlett, , # 1 art. no. D24104ST, p. 170 - 172
反应条件
thionyl chloride in dichloromethane T=20°C; 0.75 h; other reagents (SCl2, S2Cl2) and time; Product distribution;
参考文献
Gazzetta Chimica Italiana, , vol. 111, # 7/8 p. 289 - 292
反应条件
benzeneseleninic anhydride in tetrahydrofuran 0.666667 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Lester, David J.; Ley, Steven V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1212 - 1217
反应条件
sodium acetate; bis(benzoyloxy)borane in chloroform T=0°C; 1 h;
参考文献
Kabalka, George W.; Summers, Timothy S.
Journal of Organic Chemistry, 1981 , vol. 46, p. 1217 - 1218
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water T=20°C; Oxidation; oxidative cleavage; 2 h;
参考文献
Chemistry Letters, , # 4 p. 430 - 431
反应条件
copper(l) iodide; caesium carbonate in ethylene glycol dimethyl ether
T=80°C; 12 h; Inert atmosphere;
参考文献
Miao, Wenjun; Gao, Yuzhen; Li, Xueqin; Gao, Yuxing; Tang, Guo; Zhao, Yufen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2659 - 2664