2,2-二氯-2,2a,7,7a-四氢-1H-环丁[a]茚-1-酮合成路线 (共 3 条)
反应条件
acetic acid; triethylamine in acetone
参考文献
Brady,W.T.; Hieble,J.P.
Journal of the American Chemical Society, 1972 , vol. 94, p. 4278 - 4284
参考文献
Journal of the American Chemical Society, , vol. 102, # 16 p. 5265 - 5273
反应条件
1: ammonium chloride, zinc / methanol / 40 h / Heating
2: 77 percent / 1.1 M tetrabutylammonium fluoride / tetrahydrofuran / 3 h / 20 °C
3: 89 percent / AIBN, tributylstannane / cyclohexane / 4 h / Heating
View Scheme
参考文献
Boivin, Jean; Fouquet, Eric; Zard, Samir Z.
Tetrahedron, 1994 , vol. 50, # 6 p. 1757 - 1768