2,3-环氧丙基膦酸二乙基酯合成路线 (共 23 条)
反应条件
copper(l) iodide in tetrahydrofuran T=0°C; 2 h;
参考文献
Phillips, A. M. M. M.; Mphahlele, M. J.; Modro, A. M.; Modro, T. A.; Zwierzak, A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 71, p. 165 - 174
反应条件
copper(l) iodide in tetrahydrofuran T=-30 - 0°C; 2 h;
参考文献
Gajda, T.; Nowalinska, M.; Zawadzki, S.; Zwierzak, A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 105, # 1-4 p. 45 - 50
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; 51 h; Cooling with ice;
参考文献
Mitula, Pawel; Wawrzenczyk, Czeslaw
Arkivoc, 2012 , vol. 2012, # 4 p. 216 - 232
反应条件
1) 130 deg C, 4 h, 2) 150 deg C, 1 h;
参考文献
Masschelein, Kurt G. R.; Stevens, Christian V.
Journal of Organic Chemistry, 2007 , vol. 72, # 24 p. 9248 - 9252
参考文献
Arbusow; Lugowkin
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 1193,1198; engl. Ausg. S. 1241, 1245
反应条件
copper(l) iodide in diethyl ether; hexane
T=0°C; 3 h;
参考文献
Phillips, A. M. M. M.; Mphahlele, M. J.; Modro, A. M.; Modro, T. A.; Zwierzak, A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 71, p. 165 - 174
反应条件
copper(l) iodide in tetrahydrofuran
T=-30 - 0°C; 2 h;
参考文献
Gajda, T.; Nowalinska, M.; Zawadzki, S.; Zwierzak, A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 105, # 1-4 p. 45 - 50
反应条件
copper(l) iodide in tetrahydrofuran
T=-30 - 0°C; 2 h;
参考文献
Gajda, T.; Nowalinska, M.; Zawadzki, S.; Zwierzak, A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 105, # 1-4 p. 45 - 50
参考文献
Rohm and Hass Company
Patent: US4693742 A1, 1987 ;
反应条件
copper(l) iodide in tetrahydrofuran
T=-30 - 0°C; 2 h;
参考文献
Gajda, T.; Nowalinska, M.; Zawadzki, S.; Zwierzak, A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 105, # 1-4 p. 45 - 50