1: CH2Cl2 / 2 h / Ambient temperature
2: 75 percent / DBU / CCl4 / 0.08 h / 0 °C
3: MCPBA / CH2Cl2 / -78 °C
4: 6.4 percent Spectr. / 220 - 230 °C / 14 Torr
View Scheme
参考文献
Fleming, Ian; Goldhill, Jon; Perry, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1563 - 1570
Fleming, Ian; Goldhill, Jon; Perry, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1563 - 1570
1: MCPBA / CH2Cl2 / -78 °C
2: 72 percent Spectr. / 120 °C / 14 Torr
View Scheme
参考文献
Fleming, Ian; Goldhill, Jon; Perry, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1563 - 1570
Stepanov, I. V.; Burmakov, A. I.; Kunshenko, B. V.; Alekseeva, L. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 244 - 248
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 2 p. 273 - 279
Stepanov, I. V.; Burmakov, A. I.; Kunshenko, B. V.; Alekseeva, L. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 244 - 248
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 2 p. 273 - 279
Stepanov, I. V.; Burmakov, A. I.; Kunshenko, B. V.; Alekseeva, L. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 244 - 248
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 2 p. 273 - 279
potassium phosphate; secondary alcohol dehydrogenase from Nocardia fusca AKU 2123; nicotinamide adenine dinucleotide in water
T=30°C; Oxidation; pH=9.0; Enzyme kinetics;
参考文献
Xie, Sheng-Xue; Ogawa, Jun; Shimizu, Sakayu
Bioscience, Biotechnology and Biochemistry, 1999 , vol. 63, # 10 p. 1721 - 1729
