2-[2-(甲硫基)苯氧基]乙胺合成路线 （共 4 条）
反应条件
hydrogenchloride; hydrazine hydrate in 2-methoxy-ethanol T=125°C; 2 h;
参考文献
Fumagalli, Laura; Bolchi, Cristiano; Colleoni, Simona; Gobbi, Marco; Moroni, Barbara; Pallavicini, Marco; Pedretti, Alessandro; Villa, Luigi; Vistoli, Giulio; Valoti, Ermanno
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2547 - 2559
反应条件
1: 64 percent / pyridine / 0 - 20 °C 2: sodium hydride / dimethylformamide / 4 h / Heating 3: 42 percent / hydrazine hydrate; HCl / 2-methoxy-ethanol / 2 h / 125 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 7 p. 2547 - 2559
反应条件
1: sodium hydride / dimethylformamide / 4 h / Heating 2: 42 percent / hydrazine hydrate; HCl / 2-methoxy-ethanol / 2 h / 125 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 7 p. 2547 - 2559
反应条件
1: 85 percent / potassium carbonate / toluene / 2 h / Heating 2: 64 percent / pyridine / 0 - 20 °C 3: sodium hydride / dimethylformamide / 4 h / Heating 4: 42 percent / hydrazine hydrate; HCl / 2-methoxy-ethanol / 2 h / 125 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 7 p. 2547 - 2559
