1: phenyl-magnesium chloride With titanium tetraethoxide in tetrahydrofuran T=0°C; 2: 1-Bromo-4-pentanoylbenzene With 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=-10°C; 6 h; Further stages.;
参考文献
Manolikakes, Georg; Dastbaravardeh, Navid; Knochel, Paul
Synlett, 2007 , # 13 p. 2077 - 2080
potassium hydroxide; hydrazine hydrate in diethylene glycol 130 deg C, 2 h then 200 deg C, 2 h;
参考文献
Gray, George W.; Hird, Michael; Lacey, David; Toyne, Kenneth J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 2041 - 2054