(S)-4-氧代-2-氮杂环丁烷羧酸苄酯合成路线 (共 4 条)
反应条件
1: With chloro-trimethyl-silane; triethylamine in diethyl ether T=0°C; 1 h; 2: With 1,1-dimethylethylmagnesium chloride in diethyl ether T=-5 - 0°C; 2 h;
参考文献
US7202279 B1, ;
Page/Page column 45 ;
反应条件
1,1-dimethylethylmagnesium chloride in diethyl ether T=0°C; Yield given;
参考文献
Tetrahedron, , vol. 46, # 13/14 p. 4733 - 4748
反应条件
chloro-trimethyl-silane; tert-butylmagnesium bromide; triethylamine Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 13 p. 992 - 994
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran 14 h;
参考文献
Baldwin, Jack E.; Adlington, Robert M.; Russell, Andrew T.; Smith, Marie L.
Tetrahedron, 1995 , vol. 51, # 16 p. 4733 - 4762