1H-苯并三唑-1-甲醛合成路线 （共 19 条）
反应条件
in diethyl ether T=20°C; 24 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505
反应条件
in tetrahydrofuran T=20°C; 0.15 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505
反应条件
in diethyl ether T=20°C; 48 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505
反应条件
in tetrahydrofuran T=67°C; 8 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505
反应条件
1: N-methyl-benzamide With n-butyllithium in tetrahydrofuran; hexanes
T=0°C; 1 h; Inert atmosphere;
2: 1H-benzotriazole-1-carboxaldehyde in tetrahydrofuran; hexanes
T=0 - 20°C; 12 h; Inert atmosphere;
参考文献
Pasqua, Adele E.; Crawford, James J.; Long, De-Liang; Marquez, Rodolfo
Journal of Organic Chemistry, 2012 , vol. 77, # 5 p. 2149 - 2158
反应条件
in xylene
T=138°C; 48 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505
反应条件
in tetrahydrofuran
T=70°C; 23 h;
参考文献
CONVERGENCE PHARMACEUTICALS LIMITED; BESWICK, Paul John; GLEAVE, Robert James; HACHISU, Shuji; VILE, Sadie; BERTHELEME, Nicolas; WARD, Simon E
Patent: WO2012/4604 A1, 2012 ;
Location in patent: Page/Page column 40-41 ;
WO 2012/004604 A1
反应条件
n-butyllithium in tetrahydrofuran; hexane
T=20°C; 2 h;
参考文献
Villa, Mathew V. J.; Targett, Sarah M.; Barnes, John C.; Whittingham, William G.; Marquez, Rodolfo
Organic Letters, 2007 , vol. 9, # 9 p. 1631 - 1633
反应条件
in tetrahydrofuran
T=20°C; 0.666667 h; Inert atmosphere;
参考文献
Galan, Hitos; Murillo, Maria Teresa; Sedano, Rosa; Nunez, Ana; De Mendoza, Javier; Gonzalez-Espartero, Amparo; Prados, Pilar
European Journal of Organic Chemistry, 2011 , # 20-21 p. 3959 - 3969
