1H-苯并三唑-1-甲醛合成路线 (共 19 条)
反应条件
diisopropyl-carbodiimide in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Mathieson, Jennifer E.; Crawford, James J.; Schmidtmann, Marc; Marquez, Rodolfo
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 10 p. 2170 - 2175
反应条件
in tetrahydrofuran; isopropyl alcohol T=-15 - -5°C; 0.533333 h; Inert atmosphere;
参考文献
Matheson, Mhairi; Pasqua, Adele E.; Sewell, Alan L.; Marquez, Rodolfo
Organic Syntheses, 2013 , vol. 90, p. 358 - 366
反应条件
in tetrahydrofuran T=-10°C; 0.75 h; Inert atmosphere;
参考文献
Wang, Kai-Bing; Ran, Rui-Qiao; Xiu, Shi-Dong; Li, Chuan-Ying
Organic Letters, 2013 , vol. 15, # 10 p. 2374 - 2377
反应条件
in tetrahydrofuran T=55°C; 0.75 h; Inert atmosphereGreen chemistry;
参考文献
Organic Process Research and Development, , vol. 15, # 2 p. 467 - 470
反应条件
in tetrahydrofuran T=67°C; 10 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505
反应条件
in tetrahydrofuran T=20°C; 16 h;
参考文献
Organic Letters, , vol. 12, # 7 p. 1396 - 1399
反应条件
in tetrahydrofuran T=67°C; 5 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505
反应条件
in tetrahydrofuran T=60°C; 22.5 h;
参考文献
CONVERGENCE PHARMACEUTICALS LIMITED; BESWICK, Paul John; GLEAVE, Robert James; HACHISU, Shuji; VILE, Sadie; BERTHELEME, Nicolas; WARD, Simon E
Patent: WO2012/4604 A1, 2012 ;
Location in patent: Page/Page column 43 ;
WO 2012/004604 A1
反应条件
in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Synthesis, , # 5 p. 503 - 505
反应条件
in tetrahydrofuran T=20°C; 0.3 h;
参考文献
Katritzky; Chang; Yang
Synthesis, 1995 , # 5 p. 503 - 505