5-重氮米氏酸(=5-重氮-2,2-二甲基-1,3-二氧杂环己烷-4,6-二酮)合成路线 （共 27 条）
反应条件
1: 43 percent / tetrahydrofuran; H2O / 16 - 18 °C / UV-irradiation 2: 93 percent / benzophenone / methanol / Irradiation View Scheme
参考文献
Shevchenko; Khimich; Platz; Nikolaev
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 8 p. 1213 - 1219
反应条件
in tetrahydrofuran; water T=18 - 20°C; UV-irradiation; Product distribution; Further Variations:SolventsUV wavelength;
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 6 p. 815 - 827
反应条件
in tetrahydrofuran T=18 - 20°C; 1.25 h; UV-irradiation;
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 6 p. 815 - 827
反应条件
1.16667 h; Irradiation; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 21, # 3 p. 264 - 268
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 21, # 3 p. 321 - 325
反应条件
in tetrahydrofuran; water 3.5 h; Irradiation; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 21, # 3 p. 264 - 268
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 21, # 3 p. 321 - 325
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene) in benzene
T=120°C; 36 h; Sealed tubeInert atmosphere;
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene) in benzene
T=120°C; 26 h; Sealed tubeInert atmosphere;
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
反应条件
(+/-)-2-Ethyloxirane; rhodium (II) acetate in benzene
10 h; Heating;
参考文献
Stachel, Hans-Dietrich; Schorp, Matthias; Maier, Ludwig; Dandl, Klaus
Liebigs Annalen der Chemie, 1994 , # 11 p. 1121 - 1128
反应条件
in tetrahydrofuran; water
T=16 - 18°C; UV-irradiation;
参考文献
Shevchenko; Khimich; Platz; Nikolaev
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 8 p. 1213 - 1219
反应条件
in tetrahydrofuran; water
T=18 - 20°C; UV-irradiation; Product distribution; Further Variations:SolventsUV wavelength;
参考文献
Nikolaev; Shevchenko; Platz; Khimich
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 6 p. 815 - 827
