1,3-二对甲苯基碳二酰亚胺合成路线 (共 44 条)
反应条件
iodine; triethylamine in ethyl acetate T=0 - 5°C; 0.5 h;
参考文献
Ali, Abdur Rezzak; Ghosh, Harisadhan; Patel, Bhisma K.
Tetrahedron Letters, 2010 , vol. 51, # 7 p. 1019 - 1021
反应条件
oxo(phthalocyaninato)titanium(IV) T=190°C; 144 h; Inert atmosphereNeat (no solvent);
参考文献
Darwish, Wael; Seikel, Elisabeth; Kaesmarker, Ralf; Harms, Klaus; Sundermeyer, Joerg
Dalton Transactions, 2011 , vol. 40, # 8 p. 1787 - 1794
反应条件
I2 in tetrahydrofuran under N2 atm. THF soln. (Cp2V(p-TCD)) reacted with THF soln. I2; elem. anal.;
参考文献
Pasquali, Marco; Gambarotta, Sandro; Floriani, Carlo; Chiesi-Villa, Angiola; Guastini, Carlo
Inorganic Chemistry, 1981 , vol. 20, p. 165 - 171
反应条件
bis(trichloromethyl) carbonate; triethylamine; triphenylphosphine in dichloromethane
参考文献
Wells
Synthetic Communications, 1994 , vol. 24, # 12 p. 1715 - 1719
反应条件
in benzene 2 h; Heating;
参考文献
Molina, P.; Alajarin, M.; Arques, A.; Saez, J.
Synthetic Communications, 1982 , vol. 12, # 7 p. 573 - 578
反应条件
[(4-methylphenyl)imino](triphenyl)phosphorane in benzene Heating;
参考文献
Journal of Organic Chemistry, , vol. 64, # 4 p. 1121 - 1130
反应条件
1: 65 percent / K2CO3 / CHCl3; H2O / 2.5 h / Ambient temperature 2: N-(p-tolyl)iminotriphenylphosphorane / benzene / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 4 p. 1121 - 1130
反应条件
in not given byproducts: CH3C6H4NCNC6H4CH3; treatment of iridium complex with excess of ligand at room temp.;
参考文献
Journal of the American Chemical Society, , vol. 124, # 31 p. 9010 - 9011
参考文献
Alajarin; Molina; Sanchez-Andrada; Foces-Foces
Journal of Organic Chemistry, 1999 , vol. 64, # 4 p. 1121 - 1130
反应条件
1: titanium (IV) isopropoxide; phenyl isocyanate in toluene T=20°C; 24 h; 2: 4-methyl phenyl isocyanate in toluene 24 h; Heating;
参考文献
Chemical Communications, , # 15 p. 2017 - 2019